1,000-Hour Thermal Aging
Background
The long-term use of polypropylene composites at elevated temperatures is important for many applications. The polypropylene resin in Twintex® is heat stabilized and is well suited for elevated temperature applications. Twintex® test specimens were subject to a 140°C oven for 1,000 hours. Tensile tests were performed on exposed specimens to confirm that polymer degradation did not occur.
Experimental
> Material
| Material | Product | Color | % Glass | Thickness |
| Twintex® | T PP 60 1485 | Black | 60% | 4 mm |
> Sample Preparation
Twintex® samples were prepared by molding two layers of Twintex® 2mm consolidated sheet. The consolidated sheet was placed between two, thin stainless-steel platens and heated in a 210°C press at pressure of 5 Bars. When the middle of the material reached 200°C, the molten material was transferred to a cold press and cooled to room temperature under 15 Bars pressure.
> Test Specifications
A set of test plates was placed vertically in a Blue M circulating air oven at 140°C. After aging for 1,000 hours, the plates were removed from the oven. Tensile bars were cut from the panels subjected to the thermal aging and from virgin panels. The material was tested in both primary directions. Tensile tests were performed in accordance with ASTM D639-96 at an A2LA-certified laboratory.
> Results
A set of test plates was placed vertically in a Blue M circulating air oven at 140°C. After aging for 1,000 hours, the plates were removed from the oven. Tensile bars were cut from the panels subjected to the thermal aging and from virgin panels. The material was tested in both primary directions. Tensile tests were performed in accordance with ASTM D639-96 at an A2LA-certified laboratory.
| Tensile Properties of Virgin Twintex® Panels vs. Panels Aged for 1,000 Hours at 140°C |
| | Tensile Strength | Tensile Modulus | Tensile Elongation |
| Test Direction | Warp (MPa) | Weft (MPa) | Warp (MPa) | Weft (MPa) | Warp (MPa) | Weft (MPa) |
| Virgin Panel | 318 | 316 | 12200 | 13300 | 2.89 | 2.97 |
| Aged Panel | 314 | 300 | 13800 | 13000 | 2.56 | 2.89 |
| % Change | 99% | 95% | 113% | 98% | 89% | 97% |
> Conclusion
Subjecting Twintex® to 140°C for 1,000 hours does not significantly change the tensile properties of Twintex® in either direction.